Vacuum oven to control the annealing process in alloyed nanolayers

The design and construction of a vacuum quartz cylindrical oven to diffuse two or more metallic thin films for alloying is discussed. The oven has a gas-inert ambient (Ar) anda heater plate whose temperature is controlled by means of a home-made software development in Lab View 7.0. The heater area of 10 × 5 cm² raises the temperature to 600°C over time due to the water-cooled extremes implemented. The oven is heated and controlled with a DC power supply, and a K-type thermocouple is used for monitoring the temperature with a ± 0.1°C resolution. Experiments done with the oven to obtain nanostructured AuCu alloys are detailed.

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Bibliographic Details
Main Authors: Corona,J.E, Maldonado,R.D, Oliva,A.I
Format: Digital revista
Language:English
Published: Sociedad Mexicana de Física 2007
Online Access:http://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S0035-001X2007000400013
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Description
Summary:The design and construction of a vacuum quartz cylindrical oven to diffuse two or more metallic thin films for alloying is discussed. The oven has a gas-inert ambient (Ar) anda heater plate whose temperature is controlled by means of a home-made software development in Lab View 7.0. The heater area of 10 × 5 cm² raises the temperature to 600°C over time due to the water-cooled extremes implemented. The oven is heated and controlled with a DC power supply, and a K-type thermocouple is used for monitoring the temperature with a ± 0.1°C resolution. Experiments done with the oven to obtain nanostructured AuCu alloys are detailed.