Supplementary Information: Pilot monitoring scheme of water pollutants in Important Bird and Biodiversity Areas

Table S1. Compounds studied and standard supplier. Table S2. LC-MS/MS conditions and quality parameters for the analysis of pharmaceuticals (ordered by retention time: R.T.), indicating quantification (Q) and confirmation (q) transitions, Collision Energy (C.E.), the response Factor (F) of the calibration curve, Instrument Detection Limit (IDL), Method Detection Limit (MDL), intra-day precision (%, n=5), inter-day precision (%, n=5) and percentage recovery with standard deviation (%R±SD). Coefficient of determination (R2) was 0.99 for all compounds over a concentration range of 0.001-0.6 ng/µL. Table S3. LC-MS/MS conditions and quality parameters for the analysis of pesticides and OPEs (*) (ordered by retention time: R.T.), indicating quantification (Q) and confirmation (q) transitions used, Collision Energy (C.E.), the response Factor (F) of the calibration curve, Instrument Detection Limit (IDL), Method Detection Limit (MDL), intra-day precision (%, n=5), inter-day precision (%, n=5) and percentage recovery with standard deviation (%R±SD). Coefficient of determination (R2) was 0.99 for all compounds over a concentration range of 0.001-0.6 ng/µL. Table S4. LC-MS/MS conditions and quality parameters for the analysis of PFAS (ordered by retention time: R.T.), indicating quantification (Q) and confirmation (q) transitions used, Collision Energy (C.E.), the response Factor (F) of the calibration curve, Instrument Detection Limit (IDL), Method Detection Limit (MDL), intra-day precision (%, n=5), inter-day precision (%, n=5) and percentage recovery with standard deviation (%R±SD). Coefficient of determination (R2) was 0.99 for all compounds over a concentration range of 0.001-0.6 ng/µL. Figure 1. UPLC-MS/MS chromatogram of a pharmaceuticals standard at 0.6 ng/µL. Figure 2. UPLC-MS/MS chromatogram of a pesticide and organophosphoshate ester standard at 0.6 ng/µL. Figure 3. UPLC-MS/MS chromatogram of a perfluoroalkyl substances standard at 0.6 ng/µL.

Bibliographic Details

Main Authors:	Dulsat-Masvidal, Maria, Ciudad, Carlos, Infante, Octavio, Mateo, Rafael, Lacorte Bruguera, Silvia
Format:	dataset biblioteca
Language:	English
Published:	Elsevier 2022
Online Access:	http://hdl.handle.net/10261/331296
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