Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels

Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels

8 pages, 3 figures, 5 tables.-- PMID: 15460247 [PubMed].-- Printed version published Aug 27, 2004.-- Presented at the 3rd Meeting of the Spanish Association of Chromatography and Related Techniques and the European Workshop: 3rd Waste Water Cluster, Aguadule (Almeria), Spain, Nov 19–21, 2003.

Saved in:
Bibliographic Details
Main Authors: Martínez, Elena, Gros, Meritxell, Lacorte Bruguera, Silvia, Barceló, Damià
Format: artículo biblioteca
Language:English
Published: Elsevier 2004-08-11
Subjects:Water analysis, Sediments, Mussels, Extraction methods, Polycyclic aromatic hydrocarbons,
Online Access:http://hdl.handle.net/10261/16737
Tags: Add Tag
No Tags, Be the first to tag this record!
id dig-idaea-es-10261-16737
record_format koha
spelling dig-idaea-es-10261-167372019-02-14T07:26:02Z Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels Martínez, Elena Gros, Meritxell Lacorte Bruguera, Silvia Barceló, Damià Water analysis Sediments Mussels Extraction methods Polycyclic aromatic hydrocarbons 8 pages, 3 figures, 5 tables.-- PMID: 15460247 [PubMed].-- Printed version published Aug 27, 2004.-- Presented at the 3rd Meeting of the Spanish Association of Chromatography and Related Techniques and the European Workshop: 3rd Waste Water Cluster, Aguadule (Almeria), Spain, Nov 19–21, 2003. We describe in this paper simple and robust analytical protocols to determine the 16 polycyclic aromatic hydrocarbons (PAHs) of the US Environmental Protection Agency priority list in water, sediment and mussels. For water samples, eight different solid-phase extraction (SPE) sorbents have been compared and among them, C18 provided highest recoveries and limits of detection of 0.3–15 ng/L. For lyophilized sediments, Soxhlet and ultrasonic extraction were compared, and the last one permitted to recover all analytes with highest repetitivity and was validated by analysing a certified reference material. Finally, the analysis of mussels was undertaken using Soxhlet, ultrasonic and pressurized liquid extraction (PLE) and the performance of several clean-up steps are compared. Whereas for the former two, incomplete recovery or losses of some analytes were evidenced, PLE permitted a more efficient extraction and although alkaline digestion was necessary to remove coextracted compounds, the method gave acceptable recoveries and limits of detection of 0.5–7.7 μg/kg dry mass, as for sediments. In all cases, analysis was performed by gas chromatography coupled to mass spectrometry and internal standard quantification was performed using five deuterated PAHs. Each method performance is discussed for the three matrices analysed and the paper reports advantages and disadvantages of each for their routine application in monitoring programs. This work has been supported by the CICYT Project [PPQ2001-1805-CO3-01]. Peer reviewed 2009-09-08T12:49:47Z 2009-09-08T12:49:47Z 2004-08-11 artículo http://purl.org/coar/resource_type/c_6501 Journal of Chromatography A 1047(1): 69-76 (2004) 0021-9673 http://hdl.handle.net/10261/16737 10.1016/j.chroma.2004.07.003 1873-3778 en http://dx.doi.org/10.1016/j.chroma.2004.07.003 none 22195 bytes application/pdf Elsevier
institution IDAEA ES
collection DSpace
country España
countrycode ES
component Bibliográfico
access En linea
databasecode dig-idaea-es
tag biblioteca
region Europa del Sur
libraryname Biblioteca del IDAEA España
language English
topic Water analysis
Sediments
Mussels
Extraction methods
Polycyclic aromatic hydrocarbons
Water analysis
Sediments
Mussels
Extraction methods
Polycyclic aromatic hydrocarbons
spellingShingle Water analysis
Sediments
Mussels
Extraction methods
Polycyclic aromatic hydrocarbons
Water analysis
Sediments
Mussels
Extraction methods
Polycyclic aromatic hydrocarbons
Martínez, Elena
Gros, Meritxell
Lacorte Bruguera, Silvia
Barceló, Damià
Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
description 8 pages, 3 figures, 5 tables.-- PMID: 15460247 [PubMed].-- Printed version published Aug 27, 2004.-- Presented at the 3rd Meeting of the Spanish Association of Chromatography and Related Techniques and the European Workshop: 3rd Waste Water Cluster, Aguadule (Almeria), Spain, Nov 19–21, 2003.
format artículo
topic_facet Water analysis
Sediments
Mussels
Extraction methods
Polycyclic aromatic hydrocarbons
author Martínez, Elena
Gros, Meritxell
Lacorte Bruguera, Silvia
Barceló, Damià
author_facet Martínez, Elena
Gros, Meritxell
Lacorte Bruguera, Silvia
Barceló, Damià
author_sort Martínez, Elena
title Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
title_short Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
title_full Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
title_fullStr Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
title_full_unstemmed Simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
title_sort simplified procedures for the analysis of polycyclic aromatic hydrocarbons in water, sediments and mussels
publisher Elsevier
publishDate 2004-08-11
url http://hdl.handle.net/10261/16737
work_keys_str_mv AT martinezelena simplifiedproceduresfortheanalysisofpolycyclicaromatichydrocarbonsinwatersedimentsandmussels
AT grosmeritxell simplifiedproceduresfortheanalysisofpolycyclicaromatichydrocarbonsinwatersedimentsandmussels
AT lacortebruguerasilvia simplifiedproceduresfortheanalysisofpolycyclicaromatichydrocarbonsinwatersedimentsandmussels
AT barcelodamia simplifiedproceduresfortheanalysisofpolycyclicaromatichydrocarbonsinwatersedimentsandmussels
_version_ 1777669159491993600

Similar Items