Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers

ABSTRACT Luffa Cylindrica is a tropical plant from the Cucurbitaceae family, whose fruit becomes very fibrous when fully ripened. The lignocellulosic sponges of Luffa can be suitable for use as reinforcement of epoxy matrix composites, because they have a morphology with spatial 3-D arrangement as well as are eco-friendly materials (biodegradable, and high available) and have economic advantages compared to composites reinforced with synthetic fibers derived from non-renewable sources. Surface modification of the Luffa fibers was carried out by hornification and mercerization methods and was verified by Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and X-Ray Diffraction (XRD). For the fabrication of non-biodegradable composites by hand layup technique, the sponges were impregnated with an epoxy resin based on bisphenol in a metallic mold with dimensions 150×200×3 mm3, followed by compression at 5 MPa. The dynamic modulus of the fabricated composites were measured using the nondestructive impulse excitation technique (IET), according to the ASTM E1876 standard. Bar specimens with dimensions 80×25×3 mm3 of the laminated composites were tested at room temperature, with Sonelastic® (ATCP) equipment and its associated software. Results showed that the Luffa/epoxy composites has higher loss factor and dynamic modulus when the Luffa fiber is treated before the composite fabrication. The highest Young's modulus obtained was 4.05±0.31 GPa for mercerized Luffa/epoxy. For hornificated Luffa/epoxy composite the highest loss factor and shear modulus values obtained, were 0.0337±0.003 and 1.46±0.13 GPa respectively.

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Main Authors: Quinayá,Diana Carolina Parada, D’almeida,Jose Roberto Moraes
Format: Digital revista
Language:English
Published: Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro 2017
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762017000200515
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spelling oai:scielo:S1517-707620170002005152017-09-13Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibersQuinayá,Diana Carolina ParadaD’almeida,Jose Roberto Moraes Sponge gourd lignocellulosic composite impulse excitation technique non-destructive characterization ABSTRACT Luffa Cylindrica is a tropical plant from the Cucurbitaceae family, whose fruit becomes very fibrous when fully ripened. The lignocellulosic sponges of Luffa can be suitable for use as reinforcement of epoxy matrix composites, because they have a morphology with spatial 3-D arrangement as well as are eco-friendly materials (biodegradable, and high available) and have economic advantages compared to composites reinforced with synthetic fibers derived from non-renewable sources. Surface modification of the Luffa fibers was carried out by hornification and mercerization methods and was verified by Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and X-Ray Diffraction (XRD). For the fabrication of non-biodegradable composites by hand layup technique, the sponges were impregnated with an epoxy resin based on bisphenol in a metallic mold with dimensions 150×200×3 mm3, followed by compression at 5 MPa. The dynamic modulus of the fabricated composites were measured using the nondestructive impulse excitation technique (IET), according to the ASTM E1876 standard. Bar specimens with dimensions 80×25×3 mm3 of the laminated composites were tested at room temperature, with Sonelastic® (ATCP) equipment and its associated software. Results showed that the Luffa/epoxy composites has higher loss factor and dynamic modulus when the Luffa fiber is treated before the composite fabrication. The highest Young's modulus obtained was 4.05±0.31 GPa for mercerized Luffa/epoxy. For hornificated Luffa/epoxy composite the highest loss factor and shear modulus values obtained, were 0.0337±0.003 and 1.46±0.13 GPa respectively.info:eu-repo/semantics/openAccessLaboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiroem cooperação com a Associação Brasileira do Hidrogênio, ABH2Matéria (Rio de Janeiro) v.22 n.2 20172017-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762017000200515en10.1590/s1517-707620170002.0181
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country Brasil
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libraryname SciELO
language English
format Digital
author Quinayá,Diana Carolina Parada
D’almeida,Jose Roberto Moraes
spellingShingle Quinayá,Diana Carolina Parada
D’almeida,Jose Roberto Moraes
Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
author_facet Quinayá,Diana Carolina Parada
D’almeida,Jose Roberto Moraes
author_sort Quinayá,Diana Carolina Parada
title Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
title_short Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
title_full Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
title_fullStr Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
title_full_unstemmed Nondestructive characterization of epoxy matrix composites reinforced with Luffa lignocellulosic fibers
title_sort nondestructive characterization of epoxy matrix composites reinforced with luffa lignocellulosic fibers
description ABSTRACT Luffa Cylindrica is a tropical plant from the Cucurbitaceae family, whose fruit becomes very fibrous when fully ripened. The lignocellulosic sponges of Luffa can be suitable for use as reinforcement of epoxy matrix composites, because they have a morphology with spatial 3-D arrangement as well as are eco-friendly materials (biodegradable, and high available) and have economic advantages compared to composites reinforced with synthetic fibers derived from non-renewable sources. Surface modification of the Luffa fibers was carried out by hornification and mercerization methods and was verified by Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and X-Ray Diffraction (XRD). For the fabrication of non-biodegradable composites by hand layup technique, the sponges were impregnated with an epoxy resin based on bisphenol in a metallic mold with dimensions 150×200×3 mm3, followed by compression at 5 MPa. The dynamic modulus of the fabricated composites were measured using the nondestructive impulse excitation technique (IET), according to the ASTM E1876 standard. Bar specimens with dimensions 80×25×3 mm3 of the laminated composites were tested at room temperature, with Sonelastic® (ATCP) equipment and its associated software. Results showed that the Luffa/epoxy composites has higher loss factor and dynamic modulus when the Luffa fiber is treated before the composite fabrication. The highest Young's modulus obtained was 4.05±0.31 GPa for mercerized Luffa/epoxy. For hornificated Luffa/epoxy composite the highest loss factor and shear modulus values obtained, were 0.0337±0.003 and 1.46±0.13 GPa respectively.
publisher Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
publishDate 2017
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762017000200515
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