Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles

ABSTRACT In the present work, Cu2+ substituted cobalt ferrite (Co1-xCuxFe2O4, x = 0, 0.3, 0.5, 0.7 and 1) magnetic nanopowders were synthesized via chemical co-precipitation method. The prepared powders were investigated by various characterization methods such as X-ray diffraction analysis (XRD), scanning electron microscope analysis (SEM), vibrating sample magnetometer analysis (VSM) and fourier transform infrared spectroscopy analysis (FTIR). The XRD analysis reveals that the synthesized nanopowders possess single phase centred cubic spinel structure. The average crystallite size of the particles ranging from 27-49 nm was calculated by using Debye-scherrer formula. Magnetic properties of the synthesized magnetic nanoparticles are studied by using VSM. The VSM results shows the magnetic properties such as coercivity, magnetic retentivity decreases with increase in copper substitution whereas the saturation magnetization shows increment and decrement in accordance with Cu2+ substitution in cobalt ferrite nanoparticles. SEM analysis reveals the morphology of synthesized magnetic nanoparticles. FTIR spectra of Cu2+ substituted cobalt ferrite magnetic nanoparticles were recorded in the frequency range 4000-400cm-1. The spectrum shows the presence of water adsorption and metal oxygen bonds. The adhesion nature of Cu2+ substituted cobalt ferrite magnetic nanoparticles with bacteria in reviewed results indicates that the synthesized nanoparticles could be used in biotechnology and biomedical applications.

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Main Authors: Margabandhu,M., Sendhilnathan,S., Senthilkumar,S., Gajalakshmi,D.
Format: Digital revista
Language:English
Published: Instituto de Tecnologia do Paraná - Tecpar 2016
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132016000300401
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spelling oai:scielo:S1516-891320160003004012017-01-19Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite NanoparticlesMargabandhu,M.Sendhilnathan,S.Senthilkumar,S.Gajalakshmi,D. nanoparticles Co-precipitation Cubic spinel Morphology Anti-bacterial activity ABSTRACT In the present work, Cu2+ substituted cobalt ferrite (Co1-xCuxFe2O4, x = 0, 0.3, 0.5, 0.7 and 1) magnetic nanopowders were synthesized via chemical co-precipitation method. The prepared powders were investigated by various characterization methods such as X-ray diffraction analysis (XRD), scanning electron microscope analysis (SEM), vibrating sample magnetometer analysis (VSM) and fourier transform infrared spectroscopy analysis (FTIR). The XRD analysis reveals that the synthesized nanopowders possess single phase centred cubic spinel structure. The average crystallite size of the particles ranging from 27-49 nm was calculated by using Debye-scherrer formula. Magnetic properties of the synthesized magnetic nanoparticles are studied by using VSM. The VSM results shows the magnetic properties such as coercivity, magnetic retentivity decreases with increase in copper substitution whereas the saturation magnetization shows increment and decrement in accordance with Cu2+ substitution in cobalt ferrite nanoparticles. SEM analysis reveals the morphology of synthesized magnetic nanoparticles. FTIR spectra of Cu2+ substituted cobalt ferrite magnetic nanoparticles were recorded in the frequency range 4000-400cm-1. The spectrum shows the presence of water adsorption and metal oxygen bonds. The adhesion nature of Cu2+ substituted cobalt ferrite magnetic nanoparticles with bacteria in reviewed results indicates that the synthesized nanoparticles could be used in biotechnology and biomedical applications.info:eu-repo/semantics/openAccessInstituto de Tecnologia do Paraná - TecparBrazilian Archives of Biology and Technology v.59 n.spe2 20162016-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132016000300401en10.1590/1678-4324-2016161046
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countrycode BR
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region America del Sur
libraryname SciELO
language English
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author Margabandhu,M.
Sendhilnathan,S.
Senthilkumar,S.
Gajalakshmi,D.
spellingShingle Margabandhu,M.
Sendhilnathan,S.
Senthilkumar,S.
Gajalakshmi,D.
Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
author_facet Margabandhu,M.
Sendhilnathan,S.
Senthilkumar,S.
Gajalakshmi,D.
author_sort Margabandhu,M.
title Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
title_short Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
title_full Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
title_fullStr Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
title_full_unstemmed Investigation of Structural, Morphological, Magnetic Properties and Biomedical applications of Cu2+ Substituted Uncoated Cobalt Ferrite Nanoparticles
title_sort investigation of structural, morphological, magnetic properties and biomedical applications of cu2+ substituted uncoated cobalt ferrite nanoparticles
description ABSTRACT In the present work, Cu2+ substituted cobalt ferrite (Co1-xCuxFe2O4, x = 0, 0.3, 0.5, 0.7 and 1) magnetic nanopowders were synthesized via chemical co-precipitation method. The prepared powders were investigated by various characterization methods such as X-ray diffraction analysis (XRD), scanning electron microscope analysis (SEM), vibrating sample magnetometer analysis (VSM) and fourier transform infrared spectroscopy analysis (FTIR). The XRD analysis reveals that the synthesized nanopowders possess single phase centred cubic spinel structure. The average crystallite size of the particles ranging from 27-49 nm was calculated by using Debye-scherrer formula. Magnetic properties of the synthesized magnetic nanoparticles are studied by using VSM. The VSM results shows the magnetic properties such as coercivity, magnetic retentivity decreases with increase in copper substitution whereas the saturation magnetization shows increment and decrement in accordance with Cu2+ substitution in cobalt ferrite nanoparticles. SEM analysis reveals the morphology of synthesized magnetic nanoparticles. FTIR spectra of Cu2+ substituted cobalt ferrite magnetic nanoparticles were recorded in the frequency range 4000-400cm-1. The spectrum shows the presence of water adsorption and metal oxygen bonds. The adhesion nature of Cu2+ substituted cobalt ferrite magnetic nanoparticles with bacteria in reviewed results indicates that the synthesized nanoparticles could be used in biotechnology and biomedical applications.
publisher Instituto de Tecnologia do Paraná - Tecpar
publishDate 2016
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-89132016000300401
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