Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided

Plasma nitriding of a solution annealed and aged 300 grade maraging steel was studied aiming to increase the creep resistance. The surface microhardness reached 1,140 HV, producing 50 µm layer composed of ε-Fe3N and γ'-Fe4N nitrides at the uppermost sample layer. The inner core remained unaltered presenting typical plate-like martensite microstructure of maraging steels with average microhardness of 604 HV. Surface RMS roughness in the nanometric scale increase from 52 nm to 71 nm. The continuous layer of iron nitrides seems to behave as a barrier for oxidation and for inward oxygen diffusion improving the creep resistance by reducing the steady-state creep rate (εs) in 52-65% when compared with the literature results. Dominant creep mechanism is controlled by dislocations climb. Fracture surfaces of specimens presented ductile failure consisting of equiaxed and bi-modal dimples in the fibrous zone surrounded by 45º shear lip. Nitrided sample presented a reduced ductility, associated to the hard surface layer.

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Main Authors: Reis,Adriano Gonçalves dos, Reis,Danieli Aparecida Pereira, Abdalla,Antônio Jorge, Couto,Antônio Augusto, Otubo,Jorge
Format: Digital revista
Language:English
Published: ABM, ABC, ABPol 2017
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000800002
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spelling oai:scielo:S1516-143920170008000022018-04-12Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma NitridedReis,Adriano Gonçalves dosReis,Danieli Aparecida PereiraAbdalla,Antônio JorgeCouto,Antônio AugustoOtubo,Jorge maraging creep plasma nitriding fracture Plasma nitriding of a solution annealed and aged 300 grade maraging steel was studied aiming to increase the creep resistance. The surface microhardness reached 1,140 HV, producing 50 µm layer composed of ε-Fe3N and γ'-Fe4N nitrides at the uppermost sample layer. The inner core remained unaltered presenting typical plate-like martensite microstructure of maraging steels with average microhardness of 604 HV. Surface RMS roughness in the nanometric scale increase from 52 nm to 71 nm. The continuous layer of iron nitrides seems to behave as a barrier for oxidation and for inward oxygen diffusion improving the creep resistance by reducing the steady-state creep rate (εs) in 52-65% when compared with the literature results. Dominant creep mechanism is controlled by dislocations climb. Fracture surfaces of specimens presented ductile failure consisting of equiaxed and bi-modal dimples in the fibrous zone surrounded by 45º shear lip. Nitrided sample presented a reduced ductility, associated to the hard surface layer.info:eu-repo/semantics/openAccessABM, ABC, ABPolMaterials Research v.20 suppl.2 20172017-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000800002en10.1590/1980-5373-mr-2016-0744
institution SCIELO
collection OJS
country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
tag revista
region America del Sur
libraryname SciELO
language English
format Digital
author Reis,Adriano Gonçalves dos
Reis,Danieli Aparecida Pereira
Abdalla,Antônio Jorge
Couto,Antônio Augusto
Otubo,Jorge
spellingShingle Reis,Adriano Gonçalves dos
Reis,Danieli Aparecida Pereira
Abdalla,Antônio Jorge
Couto,Antônio Augusto
Otubo,Jorge
Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
author_facet Reis,Adriano Gonçalves dos
Reis,Danieli Aparecida Pereira
Abdalla,Antônio Jorge
Couto,Antônio Augusto
Otubo,Jorge
author_sort Reis,Adriano Gonçalves dos
title Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
title_short Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
title_full Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
title_fullStr Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
title_full_unstemmed Short-term Creep Properties and Fracture Surface of 18 Ni (300) Maraging Steel Plasma Nitrided
title_sort short-term creep properties and fracture surface of 18 ni (300) maraging steel plasma nitrided
description Plasma nitriding of a solution annealed and aged 300 grade maraging steel was studied aiming to increase the creep resistance. The surface microhardness reached 1,140 HV, producing 50 µm layer composed of ε-Fe3N and γ'-Fe4N nitrides at the uppermost sample layer. The inner core remained unaltered presenting typical plate-like martensite microstructure of maraging steels with average microhardness of 604 HV. Surface RMS roughness in the nanometric scale increase from 52 nm to 71 nm. The continuous layer of iron nitrides seems to behave as a barrier for oxidation and for inward oxygen diffusion improving the creep resistance by reducing the steady-state creep rate (εs) in 52-65% when compared with the literature results. Dominant creep mechanism is controlled by dislocations climb. Fracture surfaces of specimens presented ductile failure consisting of equiaxed and bi-modal dimples in the fibrous zone surrounded by 45º shear lip. Nitrided sample presented a reduced ductility, associated to the hard surface layer.
publisher ABM, ABC, ABPol
publishDate 2017
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392017000800002
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