Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts

The purpose of this work was to investigate the influence of the hot pressing variables, namely pressure, time and temperature, on the microstructure, density and hardness in a sterling silver alloy. Powders were hot pressed under different combinations of pressures (25MPa, 35MPa and 45MPa), times (10 min, 30 min and 60 min) and temperatures (250 ºC, 300 ºC, 400 ºC, 500 ºC and 700 ºC). The microstructures of hot pressed compacts were analyzed by the means of SEM/EDS and optical microscopy. The density and hardness of specimens were assessed. The microstructure of all specimens consisted in Cu-rich precipitates of different sizes dispersed in a Ag-rich matrix. Of the variables that were examined, only temperature produced significant (p<0.05) differences in the density and hardness of the compacts. Full density of powders compacts was achieved for temperatures above 400 ºC, irrespective of the hot pressing time. A hardness peak (~120HV) was observed for the specimens hot pressed at 400 ºC.

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Main Authors: Henriques,B., Soares,D., Teixeira,J.C., Silva,F.S
Format: Digital revista
Language:English
Published: ABM, ABC, ABPol 2014
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000300018
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spelling oai:scielo:S1516-143920140003000182014-06-18Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compactsHenriques,B.Soares,D.Teixeira,J.C.Silva,F.S sterling silver powder metallurgy hot pressing microstructure density hardness The purpose of this work was to investigate the influence of the hot pressing variables, namely pressure, time and temperature, on the microstructure, density and hardness in a sterling silver alloy. Powders were hot pressed under different combinations of pressures (25MPa, 35MPa and 45MPa), times (10 min, 30 min and 60 min) and temperatures (250 ºC, 300 ºC, 400 ºC, 500 ºC and 700 ºC). The microstructures of hot pressed compacts were analyzed by the means of SEM/EDS and optical microscopy. The density and hardness of specimens were assessed. The microstructure of all specimens consisted in Cu-rich precipitates of different sizes dispersed in a Ag-rich matrix. Of the variables that were examined, only temperature produced significant (p<0.05) differences in the density and hardness of the compacts. Full density of powders compacts was achieved for temperatures above 400 ºC, irrespective of the hot pressing time. A hardness peak (~120HV) was observed for the specimens hot pressed at 400 ºC.info:eu-repo/semantics/openAccessABM, ABC, ABPolMaterials Research v.17 n.3 20142014-06-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000300018en10.1590/S1516-14392014005000022
institution SCIELO
collection OJS
country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
tag revista
region America del Sur
libraryname SciELO
language English
format Digital
author Henriques,B.
Soares,D.
Teixeira,J.C.
Silva,F.S
spellingShingle Henriques,B.
Soares,D.
Teixeira,J.C.
Silva,F.S
Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
author_facet Henriques,B.
Soares,D.
Teixeira,J.C.
Silva,F.S
author_sort Henriques,B.
title Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
title_short Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
title_full Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
title_fullStr Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
title_full_unstemmed Effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (Ag-Cu alloy) powder compacts
title_sort effect of hot pressing variables on the microstructure, relative density and hardness of sterling silver (ag-cu alloy) powder compacts
description The purpose of this work was to investigate the influence of the hot pressing variables, namely pressure, time and temperature, on the microstructure, density and hardness in a sterling silver alloy. Powders were hot pressed under different combinations of pressures (25MPa, 35MPa and 45MPa), times (10 min, 30 min and 60 min) and temperatures (250 ºC, 300 ºC, 400 ºC, 500 ºC and 700 ºC). The microstructures of hot pressed compacts were analyzed by the means of SEM/EDS and optical microscopy. The density and hardness of specimens were assessed. The microstructure of all specimens consisted in Cu-rich precipitates of different sizes dispersed in a Ag-rich matrix. Of the variables that were examined, only temperature produced significant (p<0.05) differences in the density and hardness of the compacts. Full density of powders compacts was achieved for temperatures above 400 ºC, irrespective of the hot pressing time. A hardness peak (~120HV) was observed for the specimens hot pressed at 400 ºC.
publisher ABM, ABC, ABPol
publishDate 2014
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392014000300018
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