SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO

SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO

ABSTRACT An amidoxime containing 2-phenyl-1H-benzimidazole derivative, 4-(1H-Benzoimidazol-2-yl)-N-hydroxy-benzamidine, was synthesized by conversion of nitrile group of previously synthesized 2-(4-cyanophenyl)-1H-benzimidazole by treatment with hydroxylamine under alkaline solution. Characterization of both compounds was carried out by using UV-Vis, FT-IR, 1NMR and 13C NMR, and mass spectroscopic technique. Its photophysical behavior was compared in methanol and DMSO under basic condition.

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Main Authors: Rahman,Mohammad Nahidur, Bhowmick,Rina Rani, Nurnabi,Mohammad, Molla,Ashraful Islam
Format: Digital revista
Language:English
Published: Sociedad Chilena de Química 2018
Online Access:http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072018000304047
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spelling oai:scielo:S0717-970720180003040472018-10-03SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSORahman,Mohammad NahidurBhowmick,Rina RaniNurnabi,MohammadMolla,Ashraful IslamABSTRACT An amidoxime containing 2-phenyl-1H-benzimidazole derivative, 4-(1H-Benzoimidazol-2-yl)-N-hydroxy-benzamidine, was synthesized by conversion of nitrile group of previously synthesized 2-(4-cyanophenyl)-1H-benzimidazole by treatment with hydroxylamine under alkaline solution. Characterization of both compounds was carried out by using UV-Vis, FT-IR, 1NMR and 13C NMR, and mass spectroscopic technique. Its photophysical behavior was compared in methanol and DMSO under basic condition.info:eu-repo/semantics/openAccessSociedad Chilena de QuímicaJournal of the Chilean Chemical Society v.63 n.3 20182018-01-01text/htmlhttp://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072018000304047en10.4067/s0717-97072018000304047
institution SCIELO
collection OJS
country Chile
countrycode CL
component Revista
access En linea
databasecode rev-scielo-cl
tag revista
region America del Sur
libraryname SciELO
language English
format Digital
author Rahman,Mohammad Nahidur
Bhowmick,Rina Rani
Nurnabi,Mohammad
Molla,Ashraful Islam
spellingShingle Rahman,Mohammad Nahidur
Bhowmick,Rina Rani
Nurnabi,Mohammad
Molla,Ashraful Islam
SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
author_facet Rahman,Mohammad Nahidur
Bhowmick,Rina Rani
Nurnabi,Mohammad
Molla,Ashraful Islam
author_sort Rahman,Mohammad Nahidur
title SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
title_short SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
title_full SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
title_fullStr SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
title_full_unstemmed SYNTHESIS AND CHARACTERIZATION OF AN AMIDOXIME COMPOUND WITH BENZIMIDAZOLE MOIETY AND PH SENSING BEHAVIOR UNDER BASIC CONDITION IN METHANOL AND DMSO
title_sort synthesis and characterization of an amidoxime compound with benzimidazole moiety and ph sensing behavior under basic condition in methanol and dmso
description ABSTRACT An amidoxime containing 2-phenyl-1H-benzimidazole derivative, 4-(1H-Benzoimidazol-2-yl)-N-hydroxy-benzamidine, was synthesized by conversion of nitrile group of previously synthesized 2-(4-cyanophenyl)-1H-benzimidazole by treatment with hydroxylamine under alkaline solution. Characterization of both compounds was carried out by using UV-Vis, FT-IR, 1NMR and 13C NMR, and mass spectroscopic technique. Its photophysical behavior was compared in methanol and DMSO under basic condition.
publisher Sociedad Chilena de Química
publishDate 2018
url http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072018000304047
work_keys_str_mv AT rahmanmohammadnahidur synthesisandcharacterizationofanamidoximecompoundwithbenzimidazolemoietyandphsensingbehaviorunderbasicconditioninmethanolanddmso
AT bhowmickrinarani synthesisandcharacterizationofanamidoximecompoundwithbenzimidazolemoietyandphsensingbehaviorunderbasicconditioninmethanolanddmso
AT nurnabimohammad synthesisandcharacterizationofanamidoximecompoundwithbenzimidazolemoietyandphsensingbehaviorunderbasicconditioninmethanolanddmso
AT mollaashrafulislam synthesisandcharacterizationofanamidoximecompoundwithbenzimidazolemoietyandphsensingbehaviorunderbasicconditioninmethanolanddmso
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