A concise synthetic method for 1,3,5-triazinane-2,4-dithiones

1,3,5-Triazinane-2,4-dithiones were efficiently synthesized via condensation of 2 equiv. of 1-arylthioureas with 1 equiv. of aliphatic carboxylic acids using ferric chloride hexahydrate as a catalyst. This protocol has the advantages of high yield, mild condition and simple procedure.

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Bibliographic Details
Main Authors: Li,Zheng, Cai,Hongfang, Yang,Jingya, Niu,Pengxian, Liu,Chenhui
Format: Digital revista
Language:English
Published: Sociedade Brasileira de Química 2011
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532011001000015
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Description
Summary:1,3,5-Triazinane-2,4-dithiones were efficiently synthesized via condensation of 2 equiv. of 1-arylthioureas with 1 equiv. of aliphatic carboxylic acids using ferric chloride hexahydrate as a catalyst. This protocol has the advantages of high yield, mild condition and simple procedure.