Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions

Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.

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Main Authors: Siqueira,A. B., Carvalho,C. T. de, Ionashiro,E. Y., Ionashiro,M.
Format: Digital revista
Language:English
Published: Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP 2009
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702009000200002
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spelling oai:scielo:S0100-467020090002000022010-02-08Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ionsSiqueira,A. B.Carvalho,C. T. deIonashiro,E. Y.Ionashiro,M. bivalent metals pyruvate characterization thermal behaviour Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.info:eu-repo/semantics/openAccessFundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESPEclética Química v.34 n.2 20092009-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702009000200002en10.1590/S0100-46702009000200002
institution SCIELO
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country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
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region America del Sur
libraryname SciELO
language English
format Digital
author Siqueira,A. B.
Carvalho,C. T. de
Ionashiro,E. Y.
Ionashiro,M.
spellingShingle Siqueira,A. B.
Carvalho,C. T. de
Ionashiro,E. Y.
Ionashiro,M.
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
author_facet Siqueira,A. B.
Carvalho,C. T. de
Ionashiro,E. Y.
Ionashiro,M.
author_sort Siqueira,A. B.
title Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
title_short Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
title_full Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
title_fullStr Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
title_full_unstemmed Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
title_sort synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
description Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.
publisher Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP
publishDate 2009
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702009000200002
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AT ionashiroey synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions
AT ionashirom synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions
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