Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions
Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.
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Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP
2009
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oai:scielo:S0100-467020090002000022010-02-08Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ionsSiqueira,A. B.Carvalho,C. T. deIonashiro,E. Y.Ionashiro,M. bivalent metals pyruvate characterization thermal behaviour Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds.info:eu-repo/semantics/openAccessFundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESPEclética Química v.34 n.2 20092009-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702009000200002en10.1590/S0100-46702009000200002 |
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Siqueira,A. B. Carvalho,C. T. de Ionashiro,E. Y. Ionashiro,M. |
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Siqueira,A. B. Carvalho,C. T. de Ionashiro,E. Y. Ionashiro,M. Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
author_facet |
Siqueira,A. B. Carvalho,C. T. de Ionashiro,E. Y. Ionashiro,M. |
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Siqueira,A. B. |
title |
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
title_short |
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
title_full |
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
title_fullStr |
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
title_full_unstemmed |
Synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
title_sort |
synthesis, characterization and thermal behaviour on solid pyruvates of some bivalent metal ions |
description |
Solid state M-L compounds, were M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, and thermal decomposition of the isolated compounds. |
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Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP |
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2009 |
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http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702009000200002 |
work_keys_str_mv |
AT siqueiraab synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions AT carvalhoctde synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions AT ionashiroey synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions AT ionashirom synthesischaracterizationandthermalbehaviouronsolidpyruvatesofsomebivalentmetalions |
_version_ |
1756387942010454016 |