Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides

Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides

Solid State Ln-L compounds, where Ln stands for light trivalent lanthanides (La - Gd) and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, thermal behaviour and thermal decomposition of the isolated compounds.

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Main Authors: Siqueira,A. B., Carvalho,C. T. de, Rodrigues,E. C., Ionashiro,E. Y., Bannach,G., Ionashiro,M.
Format: Digital revista
Language:English
Published: Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP 2007
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000400007
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spelling oai:scielo:S0100-467020070004000072008-01-30Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanidesSiqueira,A. B.Carvalho,C. T. deRodrigues,E. C.Ionashiro,E. Y.Bannach,G.Ionashiro,M. light lanthanides pyruvate characterization thermal behaviour Solid State Ln-L compounds, where Ln stands for light trivalent lanthanides (La - Gd) and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, thermal behaviour and thermal decomposition of the isolated compounds.info:eu-repo/semantics/openAccessFundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESPEclética Química v.32 n.4 20072007-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000400007en10.1590/S0100-46702007000400007
institution SCIELO
collection OJS
country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
tag revista
region America del Sur
libraryname SciELO
language English
format Digital
author Siqueira,A. B.
Carvalho,C. T. de
Rodrigues,E. C.
Ionashiro,E. Y.
Bannach,G.
Ionashiro,M.
spellingShingle Siqueira,A. B.
Carvalho,C. T. de
Rodrigues,E. C.
Ionashiro,E. Y.
Bannach,G.
Ionashiro,M.
Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
author_facet Siqueira,A. B.
Carvalho,C. T. de
Rodrigues,E. C.
Ionashiro,E. Y.
Bannach,G.
Ionashiro,M.
author_sort Siqueira,A. B.
title Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
title_short Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
title_full Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
title_fullStr Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
title_full_unstemmed Synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
title_sort synthesis, characterization and thermal behaviour on solid pyruvates of light trivalent lanthanides
description Solid State Ln-L compounds, where Ln stands for light trivalent lanthanides (La - Gd) and L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, ligand denticity, thermal behaviour and thermal decomposition of the isolated compounds.
publisher Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP
publishDate 2007
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000400007
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AT ionashiroey synthesischaracterizationandthermalbehaviouronsolidpyruvatesoflighttrivalentlanthanides
AT bannachg synthesischaracterizationandthermalbehaviouronsolidpyruvatesoflighttrivalentlanthanides
AT ionashirom synthesischaracterizationandthermalbehaviouronsolidpyruvatesoflighttrivalentlanthanides
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