Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees
A comparison between QuEChERS and other pesticide extraction procedures for honey and honey bee matrices is discussed. Honey bee matrix was extracted by solvent based procedure whereas solid phase extraction was the protocol for the honey matrix. The citrate buffered QuEChERS method was used for both matrices. The methods were evaluated regarding cost (equipment and reagents), time, accuracy, precision, sensitivity and versatility. The results proved that the QuEChERS protocol was the most efficient method for the extraction of the selected pesticides in both matrices. QuEChERS is the most economical and less time-consuming procedure.SPE and solvent-based extraction procedures show equivalent recoveries to QuEChERS.QuEChERS can be used to extract pesticide residues from both matrices.
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| Format: | artículo biblioteca |
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Elsevier
2016
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| Subjects: | Solvent extraction, LC–MS/MS, Pesticide, Honey bee, Honey, Solid phase extraction (SPE), QuEChERS, |
| Online Access: | http://hdl.handle.net/10261/141118 |
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dig-cide-es-10261-1411182021-12-27T15:42:39Z Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees Calatayud-Vernich, Pau Calatayud, Fernando Simó, Enrique Picó, Yolanda Universidad de Valencia Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS A comparison between QuEChERS and other pesticide extraction procedures for honey and honey bee matrices is discussed. Honey bee matrix was extracted by solvent based procedure whereas solid phase extraction was the protocol for the honey matrix. The citrate buffered QuEChERS method was used for both matrices. The methods were evaluated regarding cost (equipment and reagents), time, accuracy, precision, sensitivity and versatility. The results proved that the QuEChERS protocol was the most efficient method for the extraction of the selected pesticides in both matrices. QuEChERS is the most economical and less time-consuming procedure.SPE and solvent-based extraction procedures show equivalent recoveries to QuEChERS.QuEChERS can be used to extract pesticide residues from both matrices. This work has been supported by the agreement No. OTR2013-11072ASESO between the Agrupación de Defensa Sanitaria Apicola (apiADS) andt he Environmental and Food Safety Research Group (SAMA-UV), Department of Medicine Preventive, Faculty of Pharmacy, University of Valencia (Spain). Peer Reviewed 2016-12-02T11:40:42Z 2016-12-02T11:40:42Z 2016 2016-12-02T11:40:42Z artículo http://purl.org/coar/resource_type/c_6501 issn: 2215-0161 MethodsX 3: 452-458 (2016) http://hdl.handle.net/10261/141118 10.1016/j.mex.2016.05.005 27331025 Publisher's version https://doi.org/10.1016/j.mex.2016.05.005 Sí open Elsevier |
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Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS |
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Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS Calatayud-Vernich, Pau Calatayud, Fernando Simó, Enrique Picó, Yolanda Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| description |
A comparison between QuEChERS and other pesticide extraction procedures for honey and honey bee matrices is discussed. Honey bee matrix was extracted by solvent based procedure whereas solid phase extraction was the protocol for the honey matrix. The citrate buffered QuEChERS method was used for both matrices. The methods were evaluated regarding cost (equipment and reagents), time, accuracy, precision, sensitivity and versatility. The results proved that the QuEChERS protocol was the most efficient method for the extraction of the selected pesticides in both matrices. QuEChERS is the most economical and less time-consuming procedure.SPE and solvent-based extraction procedures show equivalent recoveries to QuEChERS.QuEChERS can be used to extract pesticide residues from both matrices. |
| author2 |
Universidad de Valencia |
| author_facet |
Universidad de Valencia Calatayud-Vernich, Pau Calatayud, Fernando Simó, Enrique Picó, Yolanda |
| format |
artículo |
| topic_facet |
Solvent extraction LC–MS/MS Pesticide Honey bee Honey Solid phase extraction (SPE) QuEChERS |
| author |
Calatayud-Vernich, Pau Calatayud, Fernando Simó, Enrique Picó, Yolanda |
| author_sort |
Calatayud-Vernich, Pau |
| title |
Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| title_short |
Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| title_full |
Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| title_fullStr |
Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| title_full_unstemmed |
Efficiency of QuEChERS approach for determining 52 pesticide residues in honey and honey bees |
| title_sort |
efficiency of quechers approach for determining 52 pesticide residues in honey and honey bees |
| publisher |
Elsevier |
| publishDate |
2016 |
| url |
http://hdl.handle.net/10261/141118 |
| work_keys_str_mv |
AT calatayudvernichpau efficiencyofquechersapproachfordetermining52pesticideresiduesinhoneyandhoneybees AT calatayudfernando efficiencyofquechersapproachfordetermining52pesticideresiduesinhoneyandhoneybees AT simoenrique efficiencyofquechersapproachfordetermining52pesticideresiduesinhoneyandhoneybees AT picoyolanda efficiencyofquechersapproachfordetermining52pesticideresiduesinhoneyandhoneybees |
| _version_ |
1777665536184811520 |