Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment.
A method for the determination of pesticide residues in water and sediment was developed using the QuEChERS method followed by gas chromatography ? mass spectrometry. The method was validated in terms of accuracy, specificity, linearity, detection and quantification limits. The recovery percentages obtained for the pesticides in water at different concentrations ranged from 63 to 116%, with relative standard deviations below 12%. The corresponding results from the sediment ranged from 48 to 115% with relative standard deviations below 16%. The limits of detection for the pesticides in water and sediment were below 0.003 mg L?1 and 0.02 mg kg?1, respectively.
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Format: | Artigo de periódico biblioteca |
Language: | Portugues pt_BR |
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2011-05-03
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Subjects: | QuEChERS method, Sediment In, pesticides, water, |
Online Access: | http://www.alice.cnptia.embrapa.br/alice/handle/doc/887438 https://doi.org/10.1007/s00128-010-0176-9 |
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dig-alice-doc-8874382022-07-22T18:19:30Z Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. BRONDI, S. H. G. MACEDO, A. N. VICENTE, G. H. L. NOGUEIRA, A. R. de A. S. H. G. BRONDI, FAPESP/SÃO CARLOS, SP; A. N. DE MACEDO, USP/SÃO CARLOS, SP; G. H. L. VICENTE, USP/SÃO CARLOS, SP; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. QuEChERS method Sediment In pesticides water A method for the determination of pesticide residues in water and sediment was developed using the QuEChERS method followed by gas chromatography ? mass spectrometry. The method was validated in terms of accuracy, specificity, linearity, detection and quantification limits. The recovery percentages obtained for the pesticides in water at different concentrations ranged from 63 to 116%, with relative standard deviations below 12%. The corresponding results from the sediment ranged from 48 to 115% with relative standard deviations below 16%. The limits of detection for the pesticides in water and sediment were below 0.003 mg L?1 and 0.02 mg kg?1, respectively. 2022-07-22T18:19:22Z 2022-07-22T18:19:22Z 2011-05-03 2011 Artigo de periódico Bulletin Environmental Contamination Toxicology, v. 86 p. 18-22, 2011. http://www.alice.cnptia.embrapa.br/alice/handle/doc/887438 https://doi.org/10.1007/s00128-010-0176-9 Portugues pt_BR openAccess |
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QuEChERS method Sediment In pesticides water QuEChERS method Sediment In pesticides water |
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QuEChERS method Sediment In pesticides water QuEChERS method Sediment In pesticides water BRONDI, S. H. G. MACEDO, A. N. VICENTE, G. H. L. NOGUEIRA, A. R. de A. Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
description |
A method for the determination of pesticide residues in water and sediment was developed using the QuEChERS method followed by gas chromatography ? mass spectrometry. The method was validated in terms of accuracy, specificity, linearity, detection and quantification limits. The recovery percentages obtained for the pesticides in water at different concentrations ranged from 63 to 116%, with relative standard deviations below 12%. The corresponding results from the sediment ranged from 48 to 115% with relative standard deviations below 16%. The limits of detection for the pesticides in water and sediment were below 0.003 mg L?1 and 0.02 mg kg?1, respectively. |
author2 |
S. H. G. BRONDI, FAPESP/SÃO CARLOS, SP; A. N. DE MACEDO, USP/SÃO CARLOS, SP; G. H. L. VICENTE, USP/SÃO CARLOS, SP; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
author_facet |
S. H. G. BRONDI, FAPESP/SÃO CARLOS, SP; A. N. DE MACEDO, USP/SÃO CARLOS, SP; G. H. L. VICENTE, USP/SÃO CARLOS, SP; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. BRONDI, S. H. G. MACEDO, A. N. VICENTE, G. H. L. NOGUEIRA, A. R. de A. |
format |
Artigo de periódico |
topic_facet |
QuEChERS method Sediment In pesticides water |
author |
BRONDI, S. H. G. MACEDO, A. N. VICENTE, G. H. L. NOGUEIRA, A. R. de A. |
author_sort |
BRONDI, S. H. G. |
title |
Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
title_short |
Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
title_full |
Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
title_fullStr |
Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
title_full_unstemmed |
Evaluation of the QuEChERS method and gas chromatography-Mass spectrometry for the analysis pesticide residues in water and sediment. |
title_sort |
evaluation of the quechers method and gas chromatography-mass spectrometry for the analysis pesticide residues in water and sediment. |
publishDate |
2011-05-03 |
url |
http://www.alice.cnptia.embrapa.br/alice/handle/doc/887438 https://doi.org/10.1007/s00128-010-0176-9 |
work_keys_str_mv |
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1756028438902210560 |