Ceramic foams porous microstructure characterization by X-ray microtomography

Knowledge of the porous structure of amorphous materials is of fundamental importance in calculating geometrical parameters such as total porosity, pore size distribution and physical parameters relating to fluid flow inside void space. The present work deals with the measurement of the microstructural parameters of porous ceramic filters. Microtomographic measurements of samples were taken using an X-ray tube. Bremsstrahlung radiation was filtered in transmission mode with a Sn filter at 58.5 and 28.3 keV and the images analyzed in two ways. The first method consisted in analyzing transepts of the images in order to calculate total porosity based on the average particle size and media linear attenuation coefficients. The second method involved a study of the images using an image analysis software, called Imago, which allows one to calculate total porosity and pore size distribution. The total measured porosity of the filter C90 was 73.8%, 71.1%, 74.4% and 71.5% by, respectively, the Arquimedes method, simple gamma ray transmission, transept analysis and analysis of the microtomographic images at 28.3 keV.

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Main Authors: Appoloni,Carlos Roberto, Fernandes,Celso Peres, Innocentini,Murilo Daniel de Mello, Macedo,Álvaro
Format: Digital revista
Language:English
Published: ABM, ABC, ABPol 2004
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392004000400008
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spelling oai:scielo:S1516-143920040004000082005-11-08Ceramic foams porous microstructure characterization by X-ray microtomographyAppoloni,Carlos RobertoFernandes,Celso PeresInnocentini,Murilo Daniel de MelloMacedo,Álvaro microstructure ceramic foams microtomography X-ray Knowledge of the porous structure of amorphous materials is of fundamental importance in calculating geometrical parameters such as total porosity, pore size distribution and physical parameters relating to fluid flow inside void space. The present work deals with the measurement of the microstructural parameters of porous ceramic filters. Microtomographic measurements of samples were taken using an X-ray tube. Bremsstrahlung radiation was filtered in transmission mode with a Sn filter at 58.5 and 28.3 keV and the images analyzed in two ways. The first method consisted in analyzing transepts of the images in order to calculate total porosity based on the average particle size and media linear attenuation coefficients. The second method involved a study of the images using an image analysis software, called Imago, which allows one to calculate total porosity and pore size distribution. The total measured porosity of the filter C90 was 73.8%, 71.1%, 74.4% and 71.5% by, respectively, the Arquimedes method, simple gamma ray transmission, transept analysis and analysis of the microtomographic images at 28.3 keV.info:eu-repo/semantics/openAccessABM, ABC, ABPolMaterials Research v.7 n.4 20042004-12-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392004000400008en10.1590/S1516-14392004000400008
institution SCIELO
collection OJS
country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
tag revista
region America del Sur
libraryname SciELO
language English
format Digital
author Appoloni,Carlos Roberto
Fernandes,Celso Peres
Innocentini,Murilo Daniel de Mello
Macedo,Álvaro
spellingShingle Appoloni,Carlos Roberto
Fernandes,Celso Peres
Innocentini,Murilo Daniel de Mello
Macedo,Álvaro
Ceramic foams porous microstructure characterization by X-ray microtomography
author_facet Appoloni,Carlos Roberto
Fernandes,Celso Peres
Innocentini,Murilo Daniel de Mello
Macedo,Álvaro
author_sort Appoloni,Carlos Roberto
title Ceramic foams porous microstructure characterization by X-ray microtomography
title_short Ceramic foams porous microstructure characterization by X-ray microtomography
title_full Ceramic foams porous microstructure characterization by X-ray microtomography
title_fullStr Ceramic foams porous microstructure characterization by X-ray microtomography
title_full_unstemmed Ceramic foams porous microstructure characterization by X-ray microtomography
title_sort ceramic foams porous microstructure characterization by x-ray microtomography
description Knowledge of the porous structure of amorphous materials is of fundamental importance in calculating geometrical parameters such as total porosity, pore size distribution and physical parameters relating to fluid flow inside void space. The present work deals with the measurement of the microstructural parameters of porous ceramic filters. Microtomographic measurements of samples were taken using an X-ray tube. Bremsstrahlung radiation was filtered in transmission mode with a Sn filter at 58.5 and 28.3 keV and the images analyzed in two ways. The first method consisted in analyzing transepts of the images in order to calculate total porosity based on the average particle size and media linear attenuation coefficients. The second method involved a study of the images using an image analysis software, called Imago, which allows one to calculate total porosity and pore size distribution. The total measured porosity of the filter C90 was 73.8%, 71.1%, 74.4% and 71.5% by, respectively, the Arquimedes method, simple gamma ray transmission, transept analysis and analysis of the microtomographic images at 28.3 keV.
publisher ABM, ABC, ABPol
publishDate 2004
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392004000400008
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AT fernandescelsoperes ceramicfoamsporousmicrostructurecharacterizationbyxraymicrotomography
AT innocentinimurilodanieldemello ceramicfoamsporousmicrostructurecharacterizationbyxraymicrotomography
AT macedoalvaro ceramicfoamsporousmicrostructurecharacterizationbyxraymicrotomography
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