Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart.
Isojuripidine was isolated from the aerial parts of Solanum astherophorum Mart. Its structure was determined using a combination of homo- (1D ¹H NMR, 13C NMR-HBBD and 13C NMR-DEPT) and heteronuclear 2D NMR techniques (¹H-¹H-COSY, ¹H-¹H-NOESY, HSQC, HMBC), and HREIMS. The unambiguous assignments of ¹H and 13C NMR data of derivatives 3-N,6-O-diacetyl-isojuripidine and 3-N-cinnamoyl-isojuripidine are described.
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Sociedade Brasileira de Química
2005
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oai:scielo:S0103-505320050008000302006-01-20Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart.Silva,Tania M. S.Costa,Rodrigo A.Oliveira,Eduardo J.Barbosa-Filho,José M.Agra,Maria F.Camara,Celso A. Solanaceae Solanum asterophorum isojuripidine Isojuripidine was isolated from the aerial parts of Solanum astherophorum Mart. Its structure was determined using a combination of homo- (1D ¹H NMR, 13C NMR-HBBD and 13C NMR-DEPT) and heteronuclear 2D NMR techniques (¹H-¹H-COSY, ¹H-¹H-NOESY, HSQC, HMBC), and HREIMS. The unambiguous assignments of ¹H and 13C NMR data of derivatives 3-N,6-O-diacetyl-isojuripidine and 3-N-cinnamoyl-isojuripidine are described.info:eu-repo/semantics/openAccessSociedade Brasileira de QuímicaJournal of the Brazilian Chemical Society v.16 n.6b 20052005-11-01info:eu-repo/semantics/othertext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532005000800030en10.1590/S0103-50532005000800030 |
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Silva,Tania M. S. Costa,Rodrigo A. Oliveira,Eduardo J. Barbosa-Filho,José M. Agra,Maria F. Camara,Celso A. |
| spellingShingle |
Silva,Tania M. S. Costa,Rodrigo A. Oliveira,Eduardo J. Barbosa-Filho,José M. Agra,Maria F. Camara,Celso A. Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| author_facet |
Silva,Tania M. S. Costa,Rodrigo A. Oliveira,Eduardo J. Barbosa-Filho,José M. Agra,Maria F. Camara,Celso A. |
| author_sort |
Silva,Tania M. S. |
| title |
Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| title_short |
Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| title_full |
Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| title_fullStr |
Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| title_full_unstemmed |
Complete ¹H and 13C NMR assignments of isojuripidine from Solanum asterophorum Mart. |
| title_sort |
complete ¹h and 13c nmr assignments of isojuripidine from solanum asterophorum mart. |
| description |
Isojuripidine was isolated from the aerial parts of Solanum astherophorum Mart. Its structure was determined using a combination of homo- (1D ¹H NMR, 13C NMR-HBBD and 13C NMR-DEPT) and heteronuclear 2D NMR techniques (¹H-¹H-COSY, ¹H-¹H-NOESY, HSQC, HMBC), and HREIMS. The unambiguous assignments of ¹H and 13C NMR data of derivatives 3-N,6-O-diacetyl-isojuripidine and 3-N-cinnamoyl-isojuripidine are described. |
| publisher |
Sociedade Brasileira de Química |
| publishDate |
2005 |
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http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532005000800030 |
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