Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar
Polystyrene/layered hydroxide salt (LHS) modified with sodium dodecyl sulfate was synthesized by in situ polymerization. The materials synthesized were characterized by gravimetry, X-ray diffraction (XRD), thermogravimetry analyses (TGA), differential scanning calorimetry (DSC) and the flammability test (FT). XRD demonstrated that synthesized nanocomposites in all compositions studied showed poor global dispersion of LHS in polystyrene. TGA showed a slight decrease in thermal stability. DSC curves showed that the glass transition temperature of polystyrene and nanocomposites were similar. The FT showed that the nanocomposite with low load of LHS exhibited good results.
Main Authors: | , , |
---|---|
Format: | Digital revista |
Language: | Portuguese |
Published: |
Sociedade Brasileira de Química
2014
|
Online Access: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000100004 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
id |
oai:scielo:S0100-40422014000100004 |
---|---|
record_format |
ojs |
spelling |
oai:scielo:S0100-404220140001000042014-02-18Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelarMoraes,Samara Boaventura deBotan,RodrigoLona,Liliane Maria Ferrareso polystyrene nanocomposites layered hydroxide salt Polystyrene/layered hydroxide salt (LHS) modified with sodium dodecyl sulfate was synthesized by in situ polymerization. The materials synthesized were characterized by gravimetry, X-ray diffraction (XRD), thermogravimetry analyses (TGA), differential scanning calorimetry (DSC) and the flammability test (FT). XRD demonstrated that synthesized nanocomposites in all compositions studied showed poor global dispersion of LHS in polystyrene. TGA showed a slight decrease in thermal stability. DSC curves showed that the glass transition temperature of polystyrene and nanocomposites were similar. The FT showed that the nanocomposite with low load of LHS exhibited good results.info:eu-repo/semantics/openAccessSociedade Brasileira de QuímicaQuímica Nova v.37 n.1 20142014-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000100004pt10.1590/S0100-40422014000100004 |
institution |
SCIELO |
collection |
OJS |
country |
Brasil |
countrycode |
BR |
component |
Revista |
access |
En linea |
databasecode |
rev-scielo-br |
tag |
revista |
region |
America del Sur |
libraryname |
SciELO |
language |
Portuguese |
format |
Digital |
author |
Moraes,Samara Boaventura de Botan,Rodrigo Lona,Liliane Maria Ferrareso |
spellingShingle |
Moraes,Samara Boaventura de Botan,Rodrigo Lona,Liliane Maria Ferrareso Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
author_facet |
Moraes,Samara Boaventura de Botan,Rodrigo Lona,Liliane Maria Ferrareso |
author_sort |
Moraes,Samara Boaventura de |
title |
Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
title_short |
Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
title_full |
Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
title_fullStr |
Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
title_full_unstemmed |
Síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
title_sort |
síntese e caracterização de nanocompósitos de poliestireno/hidroxissal lamelar |
description |
Polystyrene/layered hydroxide salt (LHS) modified with sodium dodecyl sulfate was synthesized by in situ polymerization. The materials synthesized were characterized by gravimetry, X-ray diffraction (XRD), thermogravimetry analyses (TGA), differential scanning calorimetry (DSC) and the flammability test (FT). XRD demonstrated that synthesized nanocomposites in all compositions studied showed poor global dispersion of LHS in polystyrene. TGA showed a slight decrease in thermal stability. DSC curves showed that the glass transition temperature of polystyrene and nanocomposites were similar. The FT showed that the nanocomposite with low load of LHS exhibited good results. |
publisher |
Sociedade Brasileira de Química |
publishDate |
2014 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422014000100004 |
work_keys_str_mv |
AT moraessamaraboaventurade sinteseecaracterizacaodenanocompositosdepoliestirenohidroxissallamelar AT botanrodrigo sinteseecaracterizacaodenanocompositosdepoliestirenohidroxissallamelar AT lonalilianemariaferrareso sinteseecaracterizacaodenanocompositosdepoliestirenohidroxissallamelar |
_version_ |
1756387546589298688 |