Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /

Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /

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Solid phase extraction (SPE) has become a powerful and extensively used technique in the clean up and concentration of samples for analysis in a wide variety of analytical techniques. In Forensic and Clinical Applications of Solid Phase Extraction, hands-on experts explain the principles behind SPE and provide a host of readily reproducible protocols designed to allow the reader to master his or her extraction challenges with little or no additional help. These detailed methods are particularly suited to solving extraction problems in forensic and clinical chemistry and include readily understandable explanations of such complicated ideas as the principles of pH, ion exchange, and copolymeric mechanism-enhanced SPE. Numerous actual chromatograms, based on original research and from diverse applications, demonstrate the technique and the results that can be achieved. The applications are grouped by drug types and matrices. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and avoiding known pitfalls. State-of-the-art and highly practical, Forensic and Clinical Applications of Solid Phase Extraction is a complete laboratory reference manual that will give forensic and clinical chemists at any level of expertise the ability to make clean extractions with high recoveries and effectively enhance their analytical problem-solving skills.

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Main Authors: Telepchak, Michael J. author., August, Thomas F. author., Chaney, Glynn. author., SpringerLink (Online service)
Format: Texto biblioteca
Language:eng
Published: Totowa, NJ : Humana Press : Imprint: Humana Press, 2004
Subjects:Medicine., Forensic medicine., Medicine & Public Health., Forensic Medicine.,
Online Access:http://dx.doi.org/10.1007/978-1-59259-292-0
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id KOHA-OAI-TEST:185759
record_format koha
institution COLPOS
collection Koha
country México
countrycode MX
component Bibliográfico
access En linea
En linea
databasecode cat-colpos
tag biblioteca
region America del Norte
libraryname Departamento de documentación y biblioteca de COLPOS
language eng
topic Medicine.
Forensic medicine.
Medicine & Public Health.
Forensic Medicine.
Medicine.
Forensic medicine.
Medicine & Public Health.
Forensic Medicine.
spellingShingle Medicine.
Forensic medicine.
Medicine & Public Health.
Forensic Medicine.
Medicine.
Forensic medicine.
Medicine & Public Health.
Forensic Medicine.
Telepchak, Michael J. author.
August, Thomas F. author.
Chaney, Glynn. author.
SpringerLink (Online service)
Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
description Solid phase extraction (SPE) has become a powerful and extensively used technique in the clean up and concentration of samples for analysis in a wide variety of analytical techniques. In Forensic and Clinical Applications of Solid Phase Extraction, hands-on experts explain the principles behind SPE and provide a host of readily reproducible protocols designed to allow the reader to master his or her extraction challenges with little or no additional help. These detailed methods are particularly suited to solving extraction problems in forensic and clinical chemistry and include readily understandable explanations of such complicated ideas as the principles of pH, ion exchange, and copolymeric mechanism-enhanced SPE. Numerous actual chromatograms, based on original research and from diverse applications, demonstrate the technique and the results that can be achieved. The applications are grouped by drug types and matrices. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and avoiding known pitfalls. State-of-the-art and highly practical, Forensic and Clinical Applications of Solid Phase Extraction is a complete laboratory reference manual that will give forensic and clinical chemists at any level of expertise the ability to make clean extractions with high recoveries and effectively enhance their analytical problem-solving skills.
format Texto
topic_facet Medicine.
Forensic medicine.
Medicine & Public Health.
Forensic Medicine.
author Telepchak, Michael J. author.
August, Thomas F. author.
Chaney, Glynn. author.
SpringerLink (Online service)
author_facet Telepchak, Michael J. author.
August, Thomas F. author.
Chaney, Glynn. author.
SpringerLink (Online service)
author_sort Telepchak, Michael J. author.
title Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
title_short Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
title_full Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
title_fullStr Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
title_full_unstemmed Forensic and Clinical Applications of Solid Phase Extraction [electronic resource] /
title_sort forensic and clinical applications of solid phase extraction [electronic resource] /
publisher Totowa, NJ : Humana Press : Imprint: Humana Press,
publishDate 2004
url http://dx.doi.org/10.1007/978-1-59259-292-0
work_keys_str_mv AT telepchakmichaeljauthor forensicandclinicalapplicationsofsolidphaseextractionelectronicresource
AT augustthomasfauthor forensicandclinicalapplicationsofsolidphaseextractionelectronicresource
AT chaneyglynnauthor forensicandclinicalapplicationsofsolidphaseextractionelectronicresource
AT springerlinkonlineservice forensicandclinicalapplicationsofsolidphaseextractionelectronicresource
_version_ 1756265416475279360
spelling KOHA-OAI-TEST:1857592018-07-30T23:08:21ZForensic and Clinical Applications of Solid Phase Extraction [electronic resource] / Telepchak, Michael J. author. August, Thomas F. author. Chaney, Glynn. author. SpringerLink (Online service) textTotowa, NJ : Humana Press : Imprint: Humana Press,2004.engSolid phase extraction (SPE) has become a powerful and extensively used technique in the clean up and concentration of samples for analysis in a wide variety of analytical techniques. In Forensic and Clinical Applications of Solid Phase Extraction, hands-on experts explain the principles behind SPE and provide a host of readily reproducible protocols designed to allow the reader to master his or her extraction challenges with little or no additional help. These detailed methods are particularly suited to solving extraction problems in forensic and clinical chemistry and include readily understandable explanations of such complicated ideas as the principles of pH, ion exchange, and copolymeric mechanism-enhanced SPE. Numerous actual chromatograms, based on original research and from diverse applications, demonstrate the technique and the results that can be achieved. The applications are grouped by drug types and matrices. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and avoiding known pitfalls. State-of-the-art and highly practical, Forensic and Clinical Applications of Solid Phase Extraction is a complete laboratory reference manual that will give forensic and clinical chemists at any level of expertise the ability to make clean extractions with high recoveries and effectively enhance their analytical problem-solving skills.1: Introduction to Solid Phase Extraction -- 2: Silica-Based Solid Phase Extraction -- 3: The Chemistry of Bonded Silicas -- 4: Bonded Phase Sorbent Synthesis -- 5: Strategies for the Use of Solid Phase Extraction -- 6: Optimizing Solid Phase Extraction Methods -- 7: Separation of Analytes from Their Matrices -- 8: Solid Phase Extraction Troubleshooting -- 9: Drug Methods for the Toxicology Lab -- 10: Selected Solid Phase Extraction Applications in Drug Analysis -- 11: General Methods for Drug Isolation -- 12: Chemical Derivatization -- Appendix A: Glossary -- Appendix B: Reagents -- Appendix C: Preparation of Solutions and Buffers -- Appendix D: Milliequivalent and Millimole Calculations -- Appendix E: Selected Solvent Polarity and Property Scale -- Appendix F: Buffers for Solid Phase Extraction -- Appendix I: Further Reading.Solid phase extraction (SPE) has become a powerful and extensively used technique in the clean up and concentration of samples for analysis in a wide variety of analytical techniques. In Forensic and Clinical Applications of Solid Phase Extraction, hands-on experts explain the principles behind SPE and provide a host of readily reproducible protocols designed to allow the reader to master his or her extraction challenges with little or no additional help. These detailed methods are particularly suited to solving extraction problems in forensic and clinical chemistry and include readily understandable explanations of such complicated ideas as the principles of pH, ion exchange, and copolymeric mechanism-enhanced SPE. Numerous actual chromatograms, based on original research and from diverse applications, demonstrate the technique and the results that can be achieved. The applications are grouped by drug types and matrices. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and avoiding known pitfalls. State-of-the-art and highly practical, Forensic and Clinical Applications of Solid Phase Extraction is a complete laboratory reference manual that will give forensic and clinical chemists at any level of expertise the ability to make clean extractions with high recoveries and effectively enhance their analytical problem-solving skills.Medicine.Forensic medicine.Medicine & Public Health.Forensic Medicine.Springer eBookshttp://dx.doi.org/10.1007/978-1-59259-292-0URN:ISBN:9781592592920

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